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Open Access Thesis

Keywords

Explosives--Biodegradation; Explosives--Environmental aspects; Soil pollution; Water--Pollution; Academic theses;

Abstract

As a result of munitions manufacturing and decommissioning, explosive compounds have contaminated groundwater and soils at many sites throughout the U.S. and worldwide. Three of the most commonly occurring explosive contaminants are TNT, ROX, and HMX. Many processes, biological as well as physical, have been developed to remediate the contaminated material. But feasibility studies rarely take into account the three contaminants at once. We chose four of the technologies used to remediate explosives-contaminated water and studied comparatively their effectiveness and efficiency in degrading TNT, ROX, and HMX in solution at their maximal solubilities. The chosen technologies were bacterial and fungal degradation, photocatalysis and ozonation coupled with near ultraviolet (UV) radiation. A fifth technology, electrochemical peroxidation, was chosen, which never has been utilized to degrade explosives. For the biological processes, we used two commercially available bacterial consortia and a white rot fungus, Phanerochaete chrysosporium, that has been widely studied with regard to TNT degradation. Photocatalysis and near UV ozonation of the explosives in solution were performed using a fluorescent lamp instead of a UV lamp. We also studied the degradation of a dye, Crystal Violet, using near UV ozonation and the electrochemical treatment. This compound is less resistant to degradation. All experiments were carried out over 5 days, except for electrochemical peroxidation, as it is a much faster process. In all experiments, TNT was degraded more quickly and more extensively than ROX. Similarly, RDX was degraded more quickly and more extensively than HMX. Except for the biological degradation of TNT, the biological processes did not achieve complete degradation of the explosives over the 5-day period. The physical processes did. However, the latter are much more energy demanding, and therefore more costly. Thus, eventual implementation on a full-scale of any of these processes would depend on the treatment goals for TNT, RDX, and HMX at a given site ( e.g., time constraint or extent of removal). Electrochemical peroxidation is an innovative process which destroys contaminants at a much faster rate (a matter of hours). Moreover, it is not as energy demanding as the other two oxidation processes. Nonetheless, further study is necessary to know if this is a promising technology suitable for remediation of explosives-contaminated water.

Year of Submission

1999

Degree Name

Master of Science

Department

Department of Chemistry

First Advisor

John A. Bumpus

Second Advisor

Duane E. Bartak

Third Advisor

Ira M. Simet

Comments

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Date Original

1999

Object Description

1 PDF file (69 leaves)

Language

en

File Format

application/pdf

Included in

Chemistry Commons

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