Home > Iowa Academy of Science > Journals & Newsletters > Proceedings of the Iowa Academy of Science > Volume 9 (1901) > Annual Issue
Document Type
Research
Abstract
Work leading toward the preparation of this and if possible toward one of its isomers, was commenced with work on phenol. First the phenyl acetate was made as follows: forty-one grams of phenol were taken in a distilling flask, and to this were added gradually, through a reflux condenser (in hood) twenty-eight to thirty grams (excess) of acetyl chloride. The flask was heated in a water-bath until the HC1 ceased to come off. The contents of the flask were then washed with a dilute solution of sodium hydroxide brought into a separating funnel with water, and the oil separated, dried over calcium chloride and distilled. B. p. = 195°. Yield forty grams.
Publication Date
1901
Journal Title
Proceedings of the Iowa Academy of Sciences
Volume
9
Issue
1
First Page
113
Last Page
119
Copyright
©1901 Iowa Academy of Science, Inc.
Language
en
File Format
application/pdf
Recommended Citation
Goodwin, J. G.
(1901)
"Paroxymetamethylacetophenone and Some of Its Derivatives,"
Proceedings of the Iowa Academy of Science, 9(1), 113-119.
Available at:
https://scholarworks.uni.edu/pias/vol9/iss1/19