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Document Type

Research

Abstract

A detailed study of precipitation reaction of perchlorate ion with tetraphenylarsonium chloride is reported. Optimum conditions for quantitative precipitation of perchlorate ion were determined. A gravimetric and a spectrophotometric method for perchlorate ion are proposed. The spectrophotometric method is based upon dissolution of (C6H5)4AsClO4 in acetonitrile and subsequent measurement of absorbance at 264 mμ. Results on selected samples prove both methods to be accurate and reproducible.

Publication Date

1965

Journal Title

Proceedings of the Iowa Academy of Science

Volume

72

Issue

1

First Page

117

Last Page

122

Copyright

©1965 Iowa Academy of Science, Inc.

Language

en

File Format

application/pdf

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