The Preparation and Analysis of Monobromoamine, Dibromoamine, Monochloroamine, and Nitrosylchloride

Authors

George H. Coleman, State University of IowaFollow
Gilbert E. Goheen, State University of IowaFollow

Document Type

Research

Abstract

Monobromoamine and dibromoamine were prepared in ether solution by the reaction of bromine with ammonia in ether solution at the temperature attainable with a mixture of dry ice and acetone. An ethereal solution of monochloroamine in concentration of one mole per liter was prepared by the action of sodium hypochlorite on ammonia. Pure liquid nitrosyl chloride was prepared by the action of dry hydrogen chloride with nitrosyl sulfuric acid. Apparatus and methods for the preparation, purification, and analysis of these substances were illustrated and described.

Publication Date

1936

Journal Title

Proceedings of the Iowa Academy of Science

Volume

43

Issue

1

First Page

178

Last Page

178

Copyright

©1936 Iowa Academy of Science, Inc.

Language

en

File Format

application/pdf

Recommended Citation

Coleman, George H. and Goheen, Gilbert E. (1936) "The Preparation and Analysis of Monobromoamine, Dibromoamine, Monochloroamine, and Nitrosylchloride," Proceedings of the Iowa Academy of Science, 43(1), 178-178.
Available at: https://scholarworks.uni.edu/pias/vol43/iss1/34