•  
  •  
 

Document Type

Research

Abstract

The market value of chloroplatinic acid, particularly under present conditions, is so high as to warrant a careful search for some cheaper reagent for the determination of potassium. Serullas, as early as 1831, proposed taking advantage of the insolubility of potassium perchlorate in concentrated alcoholic solutions and applying it as a reagent for the estimation of potassium. Unfortunately his proposal did not receive the attention it deserved because a convenient method for the preparation of perchloric acid had not at that time been worked out. Lately, Kreider elaborated a method for the preparation of perchloric acid in large enough quantities and in sufficient purity to attempt its use as a precipitant for potassium. Following the treatment suggested by Caspari he obtained very satisfactory results.

Publication Date

1917

Journal Title

Proceedings of the Iowa Academy of Science

Volume

24

Issue

1

First Page

547

Last Page

550

Copyright

©1917 Iowa Academy of Science, Inc.

Language

en

File Format

application/pdf

Share

COinS
 
 

To view the content in your browser, please download Adobe Reader or, alternately,
you may Download the file to your hard drive.

NOTE: The latest versions of Adobe Reader do not support viewing PDF files within Firefox on Mac OS and if you are using a modern (Intel) Mac, there is no official plugin for viewing PDF files within the browser window.